Shimadzu LC 10 20 System DataApex

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Clarity DataApex and are trademarks of DataApex Ltd Microsoft and Windows TM are. trademarks of Microsoft Corporation, DataApex reserves the right to make changes to manuals without prior notice Updated manuals can be. downloaded from www dataapex com,Shimadzu LC 10 20 System Table of Contents. 1 Shimadzu LC 10 20 System 1,2 Requirements 3,2 1 Minimal version of device firmware required 4. 3 Installation Procedure 5,3 1 Shimadzu LC 10 20 System communication 5. 3 2 Software Installation 7,3 3 Clarity Configuration 8.
3 4 Shimadzu LC 10 20 System Setup 11,3 4 1 Shimadzu LC 10 20 System Setup Setup 12. 3 4 2 Shimadzu LC 10 20 System Setup Controller 14. 4 Using the control module 16,4 1 Pump 17,4 1 1 Shimadzu LC 10 20 System Setup Pump 17. 4 1 2 Method Setup LC Gradient 19,4 1 2 1 Gradient Options 21. 4 1 3 Method Setup LC 23,4 1 4 Method Setup Advanced 26. 4 1 5 Device Monitor 27,4 1 5 1 LC Control Manual Flow 30.
4 1 6 Report Setup 31,4 2 Detector 32,4 2 1 Shimadzu LC 10 20 System Setup Detector 32. 4 2 2 Method Setup Acquisition Detector 34,4 2 2 1 Method Setup Acquisition RF Detector 36. 4 2 2 2 Method Setup Acquisition RID Detector 38,4 2 3 Method Setup Acquisition Time Program 40. 4 2 4 Method Setup Acquisition Analog Output 42,4 2 5 Device Monitor 43. 4 2 6 Report Setup 45,4 3 Autosampler 47, 4 3 1 Shimadzu LC 10 20 System Setup Autosampler 47.
4 3 2 Method Setup AS Sampler 49,4 3 2 1 Method Setup AS Sampler SIL 10Axl 51. 4 3 2 2 Method Setup AS Sampler SIL 10AF 52,4 3 3 Method Setup AS Time Program 53. 4 3 4 Method Setup AS Pretreatment 54,4 3 5 Device Monitor Shimadzu LC 10 20 System 58. 4 3 6 Report Setup 59,4 4 PDA 60, 4 4 1 Shimadzu LC 10 20 System Setup PDA Detector 60. 4 4 2 Method Setup PDA 62,4 4 3 Method Setup Acquisition 64.
4 4 4 Device Monitor 65,4 4 5 Report Setup 66,Shimadzu LC 10 20 System Table of Contents. 4 5 Thermostat 67, 4 5 1 Shimadzu LC 10 20 System Setup Thermostat 67. 4 5 2 Method Setup Thermostat Thermostat 68,4 5 3 Method Setup Thermostat Time Program 69. 4 5 4 Device Monitor 70,4 5 5 Report Setup 71,5 Troubleshooting 72. 6 Vial Plate Numbers 73,Shimadzu LC 10 20 System Table of Contents.
To facilitate the orientation in the Shimadzu LC 10 20 System manual and Clarity chromatography. station different fonts are used throughout the manual Meanings of these fonts are. Instrument blue text marks the name of the window to which the text refers. Open File italics describes the commands and names of fields in Clarity parameters that can. be entered into them or a window or dialog name when you already are in the topic describing. the window, WORK1 capitals indicates the name of the file and or directory. ACTIVE capital italics marks the state of the station or its part. The bold text is sometimes also used for important parts of the text and the name of the Clarity. station Moreover some sections are written in format other than normal text These sections are. formatted as follows,Note Notifies the reader of relevant information. Caution Warns the user of possibly dangerous or very important information. Marks the problem statement or trouble question, Description Presents more detailed information on the problem describes its causes. Solution Marks the response to the question presents a procedure how to remove it. Shimadzu LC 10 20 System 1 Shimadzu LC 10 20 System. 1 Shimadzu LC 10 20 System, This manual describes the setting of the Shimadzu LC 10 20 System. The control module enables direct control of the instrument over serial line. or LAN in case of LC 20 series, Caution The Shimadzu LC 10 20 System control module can not be combined.
with Shimadzu LC 10 20 Pump control module on a single PC where. Microsoft NET Framework is installed, Caution A single Clarity station can only control one Shimadzu LC 10 20. System This is the restriction of MIMIC libraries used to perform the. instrument control,Fig 1 Shimadzu Prominence system. As opposed to the Shimadzu LC 10 20 Pump this control module. operates the whole system including detectors autosampler thermostat. etc not just the pump but requires any of the supported controllers for. the operation of any other modules Clarity can currently control following. Controllers SCL 10Avp CBM 20A CBM 20ALite, Clarity does not control following controllers CBM 10A SCL 10A. Pumps LC 6AD LC 8A LC 10AD LC 10AS LC 10AT LC 10Ai LC. 10ADvp LC 10ATvp LC 20AT LC 20AD LC 20ADXR LC 20AB LC. Detectors SPD 10A SPD 10Ai SPD 10AV SPD 10Avi SPD 10Avp. SPD 10AVvp SPD 20A SPD 20AV RID 10A RID 20A RF 10A RF. 10Axl RF 20A RF 20Axs, Autosamplers SIL 10ADvp SIL 10AF SIL 10Axl SIL HTA SIL HTC. SIL 20A SIL 20AC SIL 20AHT SIL 20ACHT SIL 20AXR SIL. PDA Detectors SPD M10Avp SPD M20A, Shimadzu LC 10 20 System 1 Shimadzu LC 10 20 System.
Thermostats CTO 10A CTO 10AC CTO 10Avp CTO 10ACvp CTO. 10ASvp CTO 20A CTO 20AC, The list continues to extend for up to date list see the website. www dataapex com Some devices also require a firmware of particular. minimal version for proper communication with Clarity for more details. see the chapter Minimal version of device firmware required on pg 4. Devices marked with the asterisk will show in the System Configuration. dialog only after the CBM 20A Lite controller has been selected. Caution If any device from the LC 20 Prominence line is to be used with the LC. 10 line Controller it is necessary to set it to the LC 10 emulation mode. This is done for example on the LC 20AD pump on the devices display. by pressing the VP key until the CALIBRATION screen appears Then. press func key enter the password and keep pressing the func key until. OP MODE screen shows There select the correct type of the controller. installed Later in the System Configuration dialog it is necessary to set the. LC 20AD pump as LC 10AD when selecting the type of the pump in the. Shimadzu LC 10 20 System setup, The autosamplers SIL 20AHT and SIL 20ACHT marked with the circle. do not possess their specific option in the Shimadzu LC 10 20 System. Autosampler dialog In case of SIL 20AHT autosampler is present it. should be configured through SIL 20A option If the SIL 20ACHT. autosampler is present it is necessary to configure it through SIL 20AC. RID 20A RF 20A and RF 20AXS detectors must be always switched to. the LC 10 emulation mode in order to be controlled using MIMIC. libraries in Clarity, SPD M10Avp PDA detector is not supported on 64 bit Windows. RF 10AXL and RF 20AXS RF 20AXS with minimum firmware version. 2 02 fluorescence detectors can be configured as a stand alone control. module developed through Knauer company This control module for RF. 10AXL and RF 20AXS fluorescence detectors supports serial. communication via special RS232 cable p n SK 11 If the RF 20A. detector was purchased through Knauer company with special oem. firmware version it can be connected to Clarity with above mentioned. special RS232 serial cable and controlled with above mentioned specific. control module,Shimadzu LC 10 20 System 2 Requirements. 2 Requirements, Clarity installation CD ROM with LC control module p n A24 allowed.
Other parts of the system may need other modules or extensions namely. the autosampler will need the AS control module p n A26 and the PDA. Detector will need the PDA extension p n A29 to operate. Supported Shimadzu system controller see the full list of supported. controllers in the chapter Shimadzu LC 10 20 System on pg 1 The. controller is needed even for the control of standalone PDA detector. Free serial port in the PC, Note Modern computers usually have only 1 if any serial COM port installed. To use more devices requiring the RS232 port the MultiCOM adapter. p n MC01 is available, Standard RS232 compliant cross DB9F DB9F serial cable p n SK01 or. cross LAN cable p n SK08 in case of LC 20 system, Note Cables are not part of Clarity Control Module It is strongly. recommended to order required cables together with the Control Module. SCSI card for use of the SPD M10Avp PDA detector SPD M20A PDA. detector uses LAN communication, Caution It is not recommended to have installed Clarity and LabSolutions. chromatography data systems on one PC at the same time It is known. that installation respectively updating one or the other data system. jeopardizes the proper functioning of the other data system These. problems are most likely to affect Windows 10 in combination with. CBM 20A CBM 20ALite controllers, Caution It is recommended to use Adaptec SCSI cards Drivers for Adaptec s.
cards are located on Clarity installation CD ROM in directory HW. DRIVERS ASPI2 Read the README TXT file before you install the. Caution SPD M10Avp PDA detector is not supported on 64 bit Windows. Shimadzu LC 10 20 System 2 Requirements,2 1 Minimal version of device firmware required. Tab 1 Controllers, Name of Device Minimal version of firmware required. SCL 10Avp 5 33,Subcontroller 5 20,OptionBox L 3 2,Tab 2 Pumps. Name of Device Minimal version of firmware required. LC 10ADvp 5 26,LC 10ATvp 5 27,LC 10Ai 3 1,LC 10AD 3 1. LC 10AT 3 1,LC 10AS 3 1,LC 6AD 1 4,Tab 3 Autosamplers.
Name of Device Minimal version of firmware required. SIL 10ADvp 5 32,SIL HTA 6 02,SIL HTC 6 02,Tab 4 Column Ovens. Name of Device Minimal version of firmware required. CTO 10Avp 5 24,CTO 10ACvp 5 24,CTO 10ASvp 5 24,CTO 10A C 3 0. Tab 5 Detectors, Name of Device Minimal version of firmware required. SPD 10Avp 5 22,SPD 10AVvp 5 22,SPD 10Ai 3 0,SPD 10Avi 3 0. SPD 10A 3 0,SPD 10AV 3 0,RF 20A Axs 1 10,Shimadzu LC 10 20 System 3 Installation Procedure.
3 Installation Procedure,3 1 Shimadzu LC 10 20 System communication. Shimadzu LC 10 20 System may be controlled either via standard serial. cross DB9F DB9F cable or via cross LAN cable depending on the type of. connector present on the controller LAN communication is only present. on LC 20 line controllers,Serial Connection, The Shimadzu LC 10 20 System is controlled by serial RS232. communication It uses standard serial cross DB9F DB9F cable described. in the picture,Fig 2 Serial cross DB9F DB9F cable,LAN connection. For direct connection between chromatograph and computer the cross. LAN cable should be used On the other hand for the connection to the. network the straight LAN cable might be necessary with older switches. Shimadzu SCL 10Avp settings, In the controller it is necessary to set the Classvp parameter accessible. from the main menu via the system submenu key 4 it is located on the. bottom of the list to 5 x value Other communication parameters set in the. controller should be,Interface RS 232C,Baud Rate 19200.
Level Enhanced, Caution Only COM ports up to COM9 are supported Serial ports with higher. numbers cannot be used This also means that the Shimadzu LC 10 20. System cannot be connected to the serial port on Net PAD COM101. and COM102,Shimadzu LC 10 20 System 3 Installation Procedure. LC 20 components with SCL 10Avp controller, Shimadzu LC 20 components have to be set to the LC 10 emulation. mode when they should be working under the LC 10 controller This is. done from the device s keyboard according to this procedure procedure. presented on the LC 20 series pump may differ slightly for other devices. Press the VP button on the devices s front keyboard until the. CALIBRATION inscription is shown on the display, Press the func button to enter the configuration The password has to be. Note The default password is 00000, Press the func button repeatedly until the OP MODE inscription is shown.
on the display, Enter the desired number 1 for the pump to switch the device to the SCL. 10Avp emulation mode and press the enter button, Switch the device off and on again The new communication parameters. should be saved and used, The procedure is in detail described in the LC 20 hardware manual. provided by the Shimadzu company,CBM 20A Lite settings. It is necessary to set the communication parameters in the controller From. Clarity version 2 6 5 the parameters are,Communication Mode ClassVP.
Interface RS232 Ethernet depending on the desired connection type. The exact procedure is described in the controllers hardware manual. Shimadzu LC 10 20 System 3 Installation Procedure,3 2 Software Installation. Caution If the PDA detector is to be used it is necessary to switch it on before the. computer is turned on This way the SCSI controller will be detected. automatically When turned on later the PDA has to be added manually. using the Add Hardware function from the Windows Control Panel. Install or re install the Clarity software from the installation CD. Insert the installation CD into the CD ROM of the computer and start the. installation, Select the target directory and press the Next button. Select Custom installation The control module for the Shimadzu LC. 10 20 System is automatically included in it, If the PDA detector is to be used select the Detector Control option its. icon is checked but grayed and either click the checkbox to change it to. checked not grayed state or press the Details button and check the. Shimadzu PDA option there, Follow the instructions given by the installation procedure until the. SHIMADZULC 10 20 SYSTEM ClarityControlModule ENG Code Rev M108 80B Date 11 27 2019 Phone 420251013400 DataApexLtd Fax 420251013401 Petrzilkova2583 13

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